Hellow guys, Welcome to my website, and you are watching How to Make 7-OH - The Oxone Method - READ THE DESCRIPTION!. and this vIdeo is uploaded by Kalifornia Kratom at 2025-09-10T18:43:52-07:00. We are pramote this video only for entertainment and educational perpose only. So, I hop you like our website.
| Name | How to Make 7-OH - The Oxone Method - READ THE DESCRIPTION! |
| Video Uploader | Video From Kalifornia Kratom |
| Upload Date | This Video Uploaded At 11-09-2025 01:43:52 |
| Video Discription | This educational video shows another method for making 7-OH, the oxone method. This is how most manufacturers make 7-OH. This video simply explains how it's made. Please don't spread your fear mongering BS on my video's comment thread, make your own video. Hateful comments and shilling will be removed - I have the power to remove comments. Items used: Separatory funnel, beakers, weigh boats, digital scale, magnetic stirrer, ring stand, scoopula, razor blade, glass dish, kratom extract, Oxone, Acetone, Baking Soda, Ethyl Acetate, and water. (Available as a kit - email matt@kaliforniakratom.com for more info) After the whole process, the product can be purified using column chromatography with silica 60 as the stationary phase, and a mixture of hexane and ethyl acetate as the mobile phase in a 3:2 ratio, respectively. 7-OH will elute last. If you don't want to use hexane, you can substitute with limonene (an oil obtained from citrus fruit peels). Oxone is a much greener alternative to using hypervalent iodine species or heavy metals as oxidation catalysts. Oxone is a mixture of peroxymonosulfate salts and is typically used as a non-chlorine oxidizing agent to clean pool water. Some people will say "oh no! you're using pool shock to oxidize mit!" These are the same people that use caustic and toxic reagents to extract mitragynine from kratom in the first place. Process: We start by adding 25 grams of extract to a beaker and diluting it to 250 mL with acetone and putting it in the refrigerator. We then dilute 25 grams of baking soda to 250 mL and add that to the refrigerator. Then we add 6 grams of oxone to 50mL of water and refrigerate that too. Then we setup our magnetic stirrer with a separatory funnel hanging from above. We add the baking soda solution to the crude extract solution and while stirring, add the oxone solution dropwise from the separatory funnel over the course of 15 minutes. Once the oxone solution is added, we let the reaction mixture stir for an additional 15 minutes before placing the beaker back into the refrigerator. After 1-2 hours, we dilute our reaction mixture by a factor of 2, and extract the alkaloids using ethyl acetate. We then wash the EA with brine solution, and transfer it into a baking dish to evaporate off the EA in a food dehydrator. We are left with several grams of a yellow-orange crystalline substance consisting of over 50% 7-OH, and mitragynine, which can then be transferred to a chromatography column for further refinement. |
| Category | Science & Technology |
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